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ULTRA-MINT Technologies - UPB
University POLITEHNICA of Bucharest
Short link:
https://eeris.eu/
ERIF-2000-000X-0650
790
Visits
Ultrasound/Microwave non-conventional technologies for activation chemical and non-chemical processes
Ioan
Calinescu
ioan.calinescu@upb.ro
PhD. eng.
SCIENTIFIC TEAM
7
Ioan CALINESCU
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Petre CHIPURICI
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Aurel DIACON
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Adina-Ionuta GAVRILA
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Vasile LAVRIC
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Adrian TRIFAN
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Mircea VINATORU
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Analytical Facilities
RI Domain of activity
Materials Synthesis or Testing Facilities
RI Domain of activity
Pilot Plants for Process Testing
RI Domain of activity
Nanotechnologies using green chemistry
RI Domain of activity
Research Data Management Plan:
No information available
Access Policy to Research Infrastructure and Related Services:
No information available
Research Services
Bioresource technology expertise
SERVICE DESCRIPTION:
New biofuels: BioDME, DMF, algal BioDiesel, Bioethanol (from celulose) Essential principles extraction from plants (enhanced in microwave field) Separation and concentration determination of complex organic mixures: polyphenols, fuels (diesel, biodiesel, gasoline) essential oils - by GC, HPLC, LC-MS/MS analysis
SERVICE PERSONS:
Adrian TRIFAN
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Aurel DIACON
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Ioan CALINESCU
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Mircea VINATORU
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Microwave green chemistry
SERVICE DESCRIPTION:
Microwave synthesis of organic compounds, extraction of active principles from plants, synthesis/activation of catalysts
SERVICE PERSONS:
Adrian TRIFAN
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Aurel DIACON
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Fischer-Tropsch synthesis
SERVICE DESCRIPTION:
Fischer-Tropsch synthesis (laboratory and pilot scale)
SERVICE PERSONS:
Adrian TRIFAN
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Silver Nanoparticle Synthesis
SERVICE DESCRIPTION:
we provide control of nanoparticle size and long term stability of silver nanoparticle
SERVICE PERSONS:
Adrian TRIFAN
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Aurel DIACON
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Ioan CALINESCU
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Complex analytical analysis
SERVICE DESCRIPTION:
Separation and concentration determination of complex organic mixures: polyphenols, fuels (diesel, biodiesel, gasoline) essential oils - by GC, HPLC, LC-MS/MS analysis
SERVICE PERSONS:
Adrian TRIFAN
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ULTRAMINT Technologies
SERVICE DESCRIPTION:
Non-conventional technologies with Ultrasound/Microwave applied for chemical and non-chemical activation of processes
SERVICE PERSONS:
Adrian TRIFAN
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Ioan CALINESCU
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Mircea VINATORU
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Vasile LAVRIC
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Petre CHIPURICI
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Adina-Ionuta GAVRILA
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Research Equipment
Gas cromatograph #1 (Buck - EPA Methods)
CATALOG NAME:
Buck Scientific 910
DESCRIPTION:
Environmental Sampling (Purge and Trap Module - EPA5030_method) Separation and quantification of liquid organic samples Detection: FID, PID, DELCD
PRODUCER:
Buck Scientific
PRODUCTION YEAR:
2005
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Gas cromatograph #2 (Buck - gas samples)
CATALOG NAME:
Buck Scientific 910
DESCRIPTION:
Separation and quantification of gas samples (CO, CO2, N2, O2, H2, C1-C6 hydrocarbons) Detection: FID, TCD
PRODUCER:
Buck Scientific
PRODUCTION YEAR:
2005
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Gas cromatograph #3 (HP 6890)
CATALOG NAME:
HP 6890
DESCRIPTION:
Separation and quantification of organic liquid mixtures. Detector: FID (very low limits of detection, ppb)
PRODUCER:
Hewlett Packard
PRODUCTION YEAR:
2000
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Microwave reactor #1 (Initiator)
CATALOG NAME:
INITIATOR
DESCRIPTION:
Reactions in microwave multimode field. pressure and temperature programmable. 0.2-20mL microreactors. magnetic stirring. batch and continuous operation mode.
PRODUCER:
Biotage
PRODUCTION YEAR:
2010
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Flash point
CATALOG NAME:
-
DESCRIPTION:
-
PRODUCER:
-
PRODUCTION YEAR:
2012
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
HPLC
CATALOG NAME:
Jasco XXXX
DESCRIPTION:
4 modules (degasser, gradient unit with 4 solvent lines, pump, UV detector); Columns: C18 (suitable for a broad spectrum of organic compounds separation) amino (suitable for sugar separation, organic acids, etc);
PRODUCER:
Jasco
PRODUCTION YEAR:
2006
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
LC-MS/MS
CATALOG NAME:
Varian
DESCRIPTION:
Detection: Quadrupole; ESI and APCI interface; Negative and positive ion operation mode;
PRODUCER:
Varian
PRODUCTION YEAR:
2001
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Fischer-Tropsch instalation
CATALOG NAME:
-
DESCRIPTION:
Catalyst Microwave Activation
PRODUCER:
Custom instalation
PRODUCTION YEAR:
2016
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Ion Cromatograph
CATALOG NAME:
IC792Basic
DESCRIPTION:
Detectort: conductivity; Suppresion operation mode for separation of anions: chloride, bromide, nitrite, nitrate, suphite, sulphate, phosphate, etc;
PRODUCER:
Metrohm
PRODUCTION YEAR:
2009
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (191.42 kb)
UV-VIS
CATALOG NAME:
UV1240mini
DESCRIPTION:
UV-VIS spectra of liquid samples.
PRODUCER:
SHIMADZU
PRODUCTION YEAR:
2009
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (21.63 kb)
Microwave reactor #2 (Miniflow 200SS)
CATALOG NAME:
Miniflow 200SS
DESCRIPTION:
The MiniFlow 200SS is an easy-to-use microwave-assisted reactor, engineered as a system specifically designed for the laboratory use (chemistry, biochemistry etc.). There are two microwave cavities that can be used with MiniFlow: TE (transversal electric) and TM (transversal magnetic). The MiniFlow 200SS has the flexibility to meet all laboratory requirements; the system can be easily configured to perform different reactions in continuous flow or in batch.
PRODUCER:
Sairem
PRODUCTION YEAR:
2017
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (719.94 kb)
Multifunctional and modulated microwave installation
CATALOG NAME:
Custom installation
DESCRIPTION:
This custom instalation can be operated with either with 3KW microwave generator or 200W solid state generator. It include all the necesary components for autotunning, measure of direct and reflected microwave power and can handle low and high SAR.
PRODUCER:
Sairem
PRODUCTION YEAR:
2017
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (487.11 kb)
Ultrasonic processor (Vibracell VCX750)
CATALOG NAME:
Vibracell VCX750
DESCRIPTION:
High power (750W) ultrasound processing. Adjustable Power: 150-750W; operation frequency: 20kHz; Probe volume: 10-250mL; continuous or pulse operation mode.
PRODUCER:
Sonics
PRODUCTION YEAR:
2017
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (122.26 kb)
Precision syringe pump
CATALOG NAME:
Atlas Syringe pump XL
DESCRIPTION:
The Atlas Syringe Pump is a versatile volumetric dosing and/or sampling system. It allows 2 independant refilling flows, one continuous flow, reaction sampling, intelligent control of pH and temperature dependant dosing. It consists of two syringes and multi port valves and be controlled from the front panel, by a Reactor Master, an Atlas Base or PC software.
PRODUCER:
Syrris
PRODUCTION YEAR:
2017
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (1613.08 kb)
Ultrasonic bath
CATALOG NAME:
UCD300
DESCRIPTION:
Volume: 18 L; Ultrasound Power: 700 W; Frequency: 35KHz; Temperature adjusting with bilt-in microprocessor: 5-90 C degree; Timer: 0-99 min; Stainless steel basket and lid;
PRODUCER:
HILSONIC
PRODUCTION YEAR:
2017
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
LABOTRON EXTRACTION & SYNTHESIS
CATALOG NAME:
LABOTRON EXTRACTION & SYNTHESIS
DESCRIPTION:
The LABOTRON series is the generic name for a ground breaking range of integrated reactor and microwave transmission systems especially designed to carry out microwave-assisted processes in batch or in continuous flow. The LABOTRON implements SAIREM’s patented INTLI (internal transmission line) technology together with the U-waveguide. The principle of the microwave-assisted processing using INTLI is to bring, very selectively, a great quantity of energy directly inside the reaction mixture. The LABOTRON can cover a wide area of chemical processes enabling efficient and reproducible syntheses from a few grams/hour to more than 1 kg/hour.
PRODUCER:
Sairem
PRODUCTION YEAR:
2017
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (844.42 kb)
Mini Dual-Frequency Reaction cell DRC
CATALOG NAME:
DRC 4 DPP CE
DESCRIPTION:
Our single frequency Ultrasonic Reaction Cells and multiple frequency Dual-Frequency Reaction Cells are very versatile for ultrasonic processing applications. The wide assortment of Transducer Assemblies, Reaction Chambers, Generator Features, and Optional Accessories allows for flexible system configurations for a variety of applications.
PRODUCER:
Advanced Sonic Processing system, USA
PRODUCTION YEAR:
2017
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (383.82 kb)
MMM Clamp on Reactor
CATALOG NAME:
AMMM - 1000 W
DESCRIPTION:
Ultrasonic systems based on MMM (Multi-frequency, Multimode, Modulated) technology may be used as structural actuators capable of delivering high power sonic and ultrasonic energy to a large or small loads. MMM uses proprietary techniques to initiate ringing and relaxing multimode (wideband high and low frequency) mechanical oscillations in a mechanical body to produce pulse-repetitive, frequency, phase and amplitude modulated bulk-wave-excitation on that body. Every MMM system consists of: A) A Sweeping-Frequency, Adaptively Modulated Wave Form generated by an MMM Ultrasonic Power Supply (including all regulations, controls and protections); B) High Power Ultrasonic Converter(s); C) Acoustical Wave-Guide (metal bar, aluminum, titanium), which connects the ultrasonic transducer with an acoustic load, oscillating body, or resonator; D) Acoustical Load (mechanical resonating body, sonoreactor, radiating ultrasonic tool, sonotrode, test specimen, vibrating tube, vibrating sphere, a mold, solid or fluid media, etc.); E) Sensors of acoustical activity fixed on, in, or at the Acoustical Load (accelerometers, ultrasonic flux meters, cavitation detectors, laser vibrometer(s), etc.), which are creating regulation feedback between the Acoustical Load and Ultrasonic Power Supply. In most of cases the piezoelectric converter can function as the feedback element, avoiding installation of other vibrations sensors.
PRODUCER:
MPI-ultrasonics
PRODUCTION YEAR:
2018
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (10895.77 kb)
Flow reactor
CATALOG NAME:
Phoenix
DESCRIPTION:
• 450 °C, 200 bar capability safely • Homogenous and heterogeneous reactions in one reactor • From mg to kg scale synthesis without system modifi cation • New process development • Fast catalyst screening • Upgradeable for more chemistry and automation • Rapid heating and cooling without solvent limitation • Wider parameter space than microwave
PRODUCER:
Thales Nano
PRODUCTION YEAR:
2018
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (1823.9 kb)
Automated synthesis system
CATALOG NAME:
syrris
DESCRIPTION:
Atlas Sodium is an automated reactor system for round bottom flasks with overhead stirring and temperature control. It includes a Magnetic Stirrer (to 1200RPM) and a Scorpion Overhead Stirrer for viscous or heterogeneous reactions (to 800RPM). The Stacking Dry Bath and hotplate heat round bottom flasks from 50ml - 1 litre (to 280°C).
PRODUCER:
Syrris
PRODUCTION YEAR:
2018
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (279.06 kb)
Two-photon polymerization
CATALOG NAME:
M4D System
DESCRIPTION:
Direct laser writing by two-photon polymerization (2PP) of photosensitive materials is a novel technique for fast and flexible fabrication of fully three-dimensional (3D) microstructures. It is based on the photopolymerization of photo resin with femtosecond lasers. In comparison to stereolithography or 3D printing, a significantly higher resolution well below 500 nm can be achieved. Characteristics: laser wavelength = 780 nm, > 500mW; Nano positioning system = 150 mm x 150 mm x 50 mm; Bidirectional repeatability <100nm; Full system control, Process 3D CAD files.
PRODUCER:
Laser NanoFab
PRODUCTION YEAR:
2018
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Phone:
+ 4021-402 2700
Fax:
+ 4021-402 2701
POLIZU
,
1-7
,
Bucuresti
011061
,
Bucuresti - Sector 6
Romania
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[T: 1.0731, O: 543]
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