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Research Center for Pure and Applied Inorganic Chemistry
University of Bucharest
Short link:
https://eeris.eu/
ERIF-2000-000M-1482
289
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Augustin M.
Mădălan
augustin.madalan@chimie.unibuc.ro
Conf. dr.
SCIENTIFIC TEAM
2
Viorel CIRCU
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Marilena FERBINTEANU CIMPOESU
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Materials Synthesis or Testing Facilities
RI Domain of activity
Analytical Facilities
RI Domain of activity
Structural Analysis
RI Domain of activity
Research Data Management Plan:
No information available
Access Policy to Research Infrastructure and Related Services:
No information available
Research Services
Synthesis and characterisation of liquid crystalline materials
SERVICE DESCRIPTION:
SERVICE PERSONS:
Viorel CIRCU
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Structural Analysis by Single-crystal X-ray Diffraction (Rigaku R-Axis Rapid II)
SERVICE DESCRIPTION:
Access to modern structural investigation methods of inorganic, organic and organometallic compounds Services 1. Unit cell- data collection and refinement for a unit cell determination. 2. Data collection- data acquisition and data refinement. Data collection provides the first part necessary for a structural determination. 3. Full determination-a full determination implies a matrix determination, which gives the unit cell, a full data collection, necessary for the structure determination, and the data refinement which will give the final crystal structure. 4. Checking the data with CCDC data base and preparing the data for publications (figures, reports). 5. Preparing input files for further ab-initio calculation and modeling.
SERVICE PERSONS:
Marilena FERBINTEANU CIMPOESU
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Research Equipment
Nikon 50iPol polarised light microscope equipped with a Linkam THMS600 hot stage and TMS94 control processor
CATALOG NAME:
DESCRIPTION:
This equipment affords variable temperature emission spectra in solid state with an OceanOptics QE65PRO spectrometer attached to the microscope and using a Nikon Intensilight excitation source.
PRODUCER:
Nikon
PRODUCTION YEAR:
2007
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Diamond DSC Perkin Elmer instrument
CATALOG NAME:
Diamond DSC Perkin Elmer instrument
DESCRIPTION:
Differential scanning calorimetry (DSC) measurements in the -30 - 600°C range.
PRODUCER:
Perkin Elmer
PRODUCTION YEAR:
2008
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
TA Q50 TGA instrument
CATALOG NAME:
TA Q50
DESCRIPTION:
PRODUCER:
TA Instruments
PRODUCTION YEAR:
2011
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
UV-Vis-NIR JASCO V-670 spectrophotometer
CATALOG NAME:
DESCRIPTION:
electronic spectra by diffuse reflectance technique in the range 200-2700 nm
PRODUCER:
Jasco
PRODUCTION YEAR:
2008
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
LABSYS 1200
CATALOG NAME:
LABSYS 1200
DESCRIPTION:
Derivatograph (TG, DTG, DTA) in air or inerte atmosphere. Heating rate 1-50 °C/min.
PRODUCER:
Setaram France
PRODUCTION YEAR:
2007
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Single Crystal X-ray Diffractometer Rigaku R-Axis Rapid II
CATALOG NAME:
Rigaku R-Axis Rapid II
DESCRIPTION:
A compact, fully integrated high-resolution, small molecule crystallography system, the Rigaku R-AXIS RAPID II is the latest member of the RAPID family of large-area curved imaging plate (IP) X-ray diffraction systems. Its unique, curved large-area detector subtends a 2θ range of 204° at a single detector setting for maximum reciprocal space coverage. The large curved active area is advantageous because a massive solid angle of data is collected in a single exposure. While the wide dynamic range eliminates worrying about detector saturation, the curved-plate geometry of the RAPID II reduces oblique-incidence X-ray absorption effects seen with flat detectors of any kind. Curved imaging plate chemical crystallography system Imaging plate (IP) and scanner: Detector: Cylindrical IP with vertical translation axis; Radius: 127.4 mm; 2θ range: Tangential direction -60° to 144°; Active area: 460 mm x 256 mmGoniometer (Partial-χ, 3-axis goniometer): ω axis: -85° to 265° 0.002° /step, χ axis: -15° to 55° 0.0002° /step; φ axis: 360° 0.002° /step’ Sphere of confusion: ≤ 20 μm; Camera: 1/3" camera for sample alignment and observation; 70X magnification color image displayed on host computerX-ray generator: 5 kW rotating anode: MoComputer: PC with Windows®Software: CrystalClear™ automated measurement/processing software; Software for face indexing using CCD video camera; TwinSolve twinned crystal integration software; CrystalStructure™ single-crystal structure solution refinement and reporting suite
PRODUCER:
Rigaku, Japan (Rigaku Oxford Diffraction)
PRODUCTION YEAR:
2011
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (565.45 kb)
Stereo Microscope
CATALOG NAME:
Leica; Optika
DESCRIPTION:
Leica Stereomicroscope with led illuminator and Optika Microscope (Model: SZM-2; Head: Trinocular; Eyepieces: WF 10x/20 mm (high point); Objectives: Continuous increment zoom 0,7x ...4,5x; Working distance: 100 mm; Stand: Pillar stand; Illuminator: Incident and transmitted 12V/15W halogen) with Opticam camera Educational and material science applications
PRODUCER:
Leica; Optika
PRODUCTION YEAR:
2012
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
ATR with temperature controller
CATALOG NAME:
GladiATR, PIKE controller
DESCRIPTION:
FTIR accessories for different samples type and temperature control from ambient temperature up to 300oC
PRODUCER:
Pike Technologies
PRODUCTION YEAR:
2012
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (241.01 kb)
Single Crystal X-Ray Diffractometer STOE IPDS II
CATALOG NAME:
STOE IPDS II
DESCRIPTION:
The equipment is a twin system (two measuring units using the same X-ray tube - Mo, maximum power 3kW) for structural determination by X-ray diffraction on single crystal. One measuring unit is equipped with an Oxford Instruments cryocooler with liquid nitrogen for low temperature measurements.
PRODUCER:
STOE & Cie GmbH, Darmstadt , Germany
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (1149.21 kb)
Powder X-Ray Diffraction PROTO AXRD
CATALOG NAME:
AXRD Benchtop Powder Diffractometer
DESCRIPTION:
600 Watts Cu X-ray tube, NaI Scintillation Detector,
PRODUCER:
PROTO Manufacturing
PRODUCTION YEAR:
2015
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (1585.7 kb)
Circular Dichroism Spectrometer Jasco J-1500
CATALOG NAME:
J-1500 Circular Dichroism Spectrometer
DESCRIPTION:
PRODUCER:
Jasco
PRODUCTION YEAR:
2013
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (8761.48 kb)
Spectrofluorometer Jasco FP-6500
CATALOG NAME:
FP-6500 Spectrofluorometer
DESCRIPTION:
PRODUCER:
Jasco
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (221.62 kb)
UV-Visible_NIR Spectrophotomer Jasco V670
CATALOG NAME:
V-670 UV-Visible-NIR Spectrophotometer
DESCRIPTION:
PRODUCER:
Jasco
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
FTIR spectrometer Bruker Tensor 37
CATALOG NAME:
DESCRIPTION:
PRODUCER:
Bruker
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
SQUID Magnetometer S700X
CATALOG NAME:
DESCRIPTION:
SQUID Magnetometer S700X with recondensing cryostat
PRODUCER:
Cryogenic ltd.
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
CHNS Elemental Analyzer Euro EA3000
CATALOG NAME:
CHNS Elemental Analyzer Euro EA3000
DESCRIPTION:
PRODUCER:
EUROVECTOR
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Simultaneous Thermal Analyzer
CATALOG NAME:
STA 6000
DESCRIPTION:
http://www.perkinelmer.com/Content/RelatedMaterials/Brochures/BRO_STA-6000.pdf
PRODUCER:
Perkin Elmer
PRODUCTION YEAR:
2010
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Phone:
+4021305 97 30
Fax:
Șoseaua Panduri nr. 90
,
90-92
,
Bucuresti
050663
,
Bucuresti - Sector 5
Romania
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