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Chromatography and Mass Spectrometry
"Costin D. Nenitzescu" Center of Organic Chemistry of the Romanian Academy
Short link:
https://eeris.eu/
ERIF-2000-000C-0881
298
Visits
The equipments allow determining and identifying trace amounts of impurities. The identification of most organic and natural compounds is also possible by combined elemental analysis, GC-MC, LC-MS and UV-Viz spectroscopy/spectrophotometry
Victoriţa
Tecuceanu
vtecu@ccocdn.ro
Dr
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SCIENTIFIC TEAM
2
Victorita TECUCEANU
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Florina TEODORESCU
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Analytical Facilities
RI Domain of activity
Materials Synthesis or Testing Facilities
RI Domain of activity
Complex sample isolation and preparation
RI Domain of activity
Research Data Management Plan:
No information available
Access Policy to Research Infrastructure and Related Services:
No information available
Research Services
Identification and purity of organic compounds
SERVICE DESCRIPTION:
Design of methods of separation and identification of organic compounds by chromatographic methods hyphenated with mass spectrometry (GC-MS and LC-MS/MS-MS). Design of methods of quantitative determination of components in mixtures of organic compounds. Organic structures assessment by mass spectrometry and elemental analysis.
SERVICE PERSONS:
Victorita TECUCEANU
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Separation of chiral organic compounds
SERVICE DESCRIPTION:
Chromatographic separations of mixtures containing chiral compounds at analytical and semi-preparative scale by Chiral LC with micropolarimeter detector.
SERVICE PERSONS:
Florina TEODORESCU
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Electronic spectra and purity of compounds
SERVICE DESCRIPTION:
Evaluation of compounds and mixtures in solution by UV-Viz spectral analysis and determination of concentration by photocolorimetric method
SERVICE PERSONS:
Victorita TECUCEANU
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Research Equipment
Automated Elemental Analyzer
CATALOG NAME:
Elemental Combustion System
DESCRIPTION:
Automated elemental analyzer CHNS/halogene by catalytic combustion. Equipped with 24/48/72 carousel auto-sampler can work fully automated, unattended.
PRODUCER:
Costech Instruments, Italy
PRODUCTION YEAR:
2008
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
GC-MS
CATALOG NAME:
Network GC System 6890N / Inert XL MSD 5975B
DESCRIPTION:
The 5975B inert XL MSD not only scans up to 1050 u but it does so with accuracy and precision. The proprietary hyperbolic quadrupole design ensures the necessary resolution to produce classical isotope ratios and accurate mass assignment across the entire mass range; the high mass test kit provides assurance of correct mass assignments. The sensitivity and ruggedness of the 5975B MSD make it especially ideal for analyzing active compounds such as pesticides and drugs in complex matrices. The system includes the Agilent 6890N GC. Features: 5975 MSD " True hyperbolic quadrupole- maximum transmission and resolution " Thermally stable quartz quadrupole- the proprietary quadrupole can be heated up to 200° C for long-term mass axis stability " Fast scanning capability- scan rates up to 10,000 u/sec " Electron impact (EI) ionization source " 1050 u mass range- extends application space for high mass compounds
PRODUCER:
Agilent Technologies, USA
PRODUCTION YEAR:
2010
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
UV-Viz spectrophotometer
CATALOG NAME:
UV-Vis-Carry100 Bio
DESCRIPTION:
Dual beam UV-Viz spectro-photo-meter with thermostated sample-holder. Works in spectral mode and in calibrated photo-metric mode for accurate concentration measurement.
PRODUCER:
Varian Inc., USA
PRODUCTION YEAR:
2008
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
HPLC-MS system
CATALOG NAME:
Varian system 310 MS
DESCRIPTION:
HPLC dual pump analytic and preparative system with diode-array detector hyphenated with triple quadrupole MS-MS system. Can perform separations at analytical to preparative level and high performance identification of organic compounds either by simple MS with catalog "finger-print" search or by structural MS-MS by means of multiple steps fragmentation pathway.
PRODUCER:
Varian Inc., USA
PRODUCTION YEAR:
2012
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Analytical and semi-preparative HPLC system
CATALOG NAME:
HPLC Series 1100/1200
DESCRIPTION:
HPLC Agilent Technology, Series 1100/1200 equiped with: - degasser G1322A - quaternary pump G1322A - autosampler G1313A - multiwavelength detector G 1365B and - fraction collector Analyt F6 The instrument is operating with ChemStation system, online and offline
PRODUCER:
Agilent Technology, USA
PRODUCTION YEAR:
2010
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Chiral Exclusion Chromatography System
CATALOG NAME:
HPLC Agilent 1200 series with Perkin Elmer micro-Polarimeter
DESCRIPTION:
HPLC system for analytical and semi-preparative enantiomers separations consisting of: Agilent 1200 series G1322A Vacuum Degasser Agilent 1200 series G1311A Quaternary Pump Agilent 1200 series G1329A Autosampler (ALS) Agilent 1200 series G1316A Thermostatted Column Compartment Agilent 1200 series G1315D Diode Array Detector DAD Agilent 1200 series G1364C Fraction Collector Perkin Elmer micro-Polarimeter Model 341
PRODUCER:
Agilent Technologies / Perkin Elmer, USA
PRODUCTION YEAR:
2010
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Phone:
0040213167900
Fax:
0040213121601
Splaiul Independentei
,
202B
,
Bucharest
060023
,
Bucuresti - Sector 6
Romania
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