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58PCCDI2018-INCDFM - Healthcare domain
National Institute of Materials Physics
Short link:
https://eeris.eu/
ERIF-2000-000S-4386
501
Visits
The 58PCCDI2018-INCDFM infrastructure encloses the research and technological services (generated by the project activities or part of our Institute portfolio) topical for the biomedical field and offered to our project partners as well as other Institutions eager to actively push at national and international level this research/technological domain of paramount importance.
George
Stan
george_stan@infim.ro
Senior researcher rank I
SCIENTIFIC TEAM
12
Luminita AMARANDE
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Cristina BESLEAGA-STAN
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Claudiu CIOBOTARU
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Ovidiu CRISAN
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Adrian ENACHE
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Iuliana PASUK
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Traian POPESCU
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Daniela PREDOI
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Mihaela SOFRONIE
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George STAN
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Cristian Mihail TEODORESCU
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Ioana Dorina VLAICU
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Materials Synthesis or Testing Facilities
RI Domain of activity
Analytical Facilities
RI Domain of activity
Biomaterials/Nanomaterials for Healthcare
RI Domain of activity
Research Data Management Plan:
No information available
Access Policy to Research Infrastructure and Related Services:
No information available
Research Services
Determination of the electrochemical properties of materials by voltammetric methods and electrochemical impedance
SERVICE DESCRIPTION:
Electrochemical methods can be used to characterize and determine the redox properties of various materials that can later be used as support for (bio) sensors.
SERVICE PERSONS:
Adrian ENACHE
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Determination of electrocatalytic properties of materials by voltammetric methods and electrochemical impedance
SERVICE DESCRIPTION:
Electrochemical methods can be used to characterize and determine the electrocatalytic properties of various materials that can be later used in the development of fuel cells.
SERVICE PERSONS:
Adrian ENACHE
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Deposition of bioactive coatings (hydroxyapatite, bioglass) on 2D and 3D objects
SERVICE DESCRIPTION:
Fabrication of magnetron sputtered ceramic and glass coatings with osteoconductive properties for the bio-functionalization of dental, cranial, or orthopedic metallic implants.
SERVICE PERSONS:
George STAN
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Pull-out adhesion testing of thin films, coatings, varnishes, and paints
SERVICE DESCRIPTION:
Measuring the bonding strength of compact (non-porous) thin films, coatings, varnishes, and paints with dedicated testers, equipped with test elements having diameters from 2.8 to 20 mm. The method complies with ISO 4624, ASTM D 4541, EN 1542 and ASTM C633 standards.
SERVICE PERSONS:
George STAN
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Powder X-ray diffraction
SERVICE DESCRIPTION:
We perform X-ray diffraction (XRD) analyses on polycrystalline materials in parafocusing geometry. We offer identification and quantitative determination of crystalline phases in powders, bulk samples or coatings. Deeper insight into the atomic structure can be obtained by precise determination of the lattice constants (for instance their variation due to doping elements, strain, or thermal treatment), refinement of atomic positions in the unit cell, determination of the average crystallite size and preferred orientation of crystallites.
SERVICE PERSONS:
Iuliana PASUK
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Thin film X-ray diffraction
SERVICE DESCRIPTION:
We perform, isotropic, textured, or epitaxial thin films analyses, using a Bruker D8 Advance high resolution X-ray diffractometer, provided with parallel, monochromatized X-ray beam. We can perform nondestructive and precise thickness measurements of films and multilayers (crystalline or amorphous), starting from a few nanometers up to 100 nm, by X-ray reflectometry (XRR). The films should have mirror-like smoothness of the surface and interfaces. The surface and interface roughness, and films densities can be also determined. For hetero-epitaxial films: we determine the in-plain orientations, the epitaxial relationship between film and substrate or within multilayers, in-plan strain and stress, etc.
SERVICE PERSONS:
Iuliana PASUK
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Synthesis of ferromagnetic shape memory (FSMA) alloys
SERVICE DESCRIPTION:
Ferromagnetic shape memory (FSMA) alloys constitute an exciting new class of smart materials that can yield magnetically switchable strains of several percent at constant temperatures. In addition to their FSMA properties, these alloys can still be operated as conventional shape memory materials and also exhibit related superelasticity, which are both important features for use in medical devices. External controllability at constant temperatures and important strains thus make the Fe-Pd alloy, with atomic composition around 70-30%, an excellent candidate for biomedical actuation, such as surgical implant material, applying for bone prostheses, or drug delivery systems. That biomaterial undergoes, by cooling the thermo-elastic and reversible martensitic transformation (MT) from f.c.c. face-centered cubic to f.c.t. face-centered tetragonal structure. A non-thermoelastic and so irreversible martensitic transformation (IMT), f.c.t.-b.c.t. (body-centered tetragonal) may be evidenced on further cooling. The martensite start temperature is near the room temperature and may be tuned by changing the composition. While the f.c.c.-phase responsible for the MT in Fe-Pd is stable only at high temperature, it becomes generally difficult to stabilize it, as single phase, in a bulk material prepared by classical methods. Rapid solidification, by using a melt-spinning technique, is an effective processing route to obtain ribbons with a non-equilibrium structure, in which the high temperature f.c.c. structure can be frozen as single phase. In addition, in order to stabilize the f.c.t. martensite, i.e. to avoid the formation of the undesirable b.c.t. martensite, as well as to manipulate the transformation temperatures, the addition of a third alloying element (Mn,Ga,Ti) in Fe-Pd system can be used.
SERVICE PERSONS:
Mihaela SOFRONIE
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Mixed oxide technology adapted for preparation of barium titanate (BT) ceramics for biological applications
SERVICE DESCRIPTION:
Mixed oxide ceramic technology consists in several steps, the first one being the mixing of the high purity oxide or carbonate raw powders (stoichiometrically weighted) by ball milling. The next step is the synthesis of the desired compound (BT in this case) by the solid state reaction (calcination at high temperature) of the homogenously mixed raw powders. Calcined powder is grinded and sieved to obtain a submicronic powder with controlled grain distribution, which is further pressed in steel dies of different geometries, required by different applications or characterization methods. The pressed samples are then sintered in alumina crucibles to obtain dense ceramic bodies, which are further mechanically processed to the final desired dimensions. Morphological and structural characterization of calcined powders and sintered ceramics is carried out. After electrodes deposition, ceramic samples are poled by applying a high electric field (30-40kV/cm), which aligns the electric dipoles along the field direction. This is the key step which confers macroscopic piezoelectric properties to ferroelectric ceramics, otherwise with no piezoelectric response, because of the randomly oriented dipoles resulted after sintering. The final step is characterization of dielectric, ferroelectric and piezoelectric properties of ceramic materials.
SERVICE PERSONS:
Luminita AMARANDE
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Mechanochemical activation technology adapted for preparation of barium titanate (BT) ceramics for biological applications
SERVICE DESCRIPTION:
Mechanochemical activation technology consists in synthesis of the desired compound (BT in this case) by prolonged and high energy milling of high purity precursor (oxide and carbonate) powders. Mecanochemical reaction occurs at nanometric level, as a result of the very high energy developed at the strong impact of the balls with powder and jar, during the high energy milling process. Thus, the collision mechanical energy is transformed into thermal and chemical energy, resulting in synthesis of the desired compound. This type of mechanochemical reaction develops in three steps. The first one consists in grinding of raw materials grains until their amorphisation. The second step is emerging of the germs of the new material. The third step is the grain growth. High impact forces are achieved by effects of centrifugal and Coriolis forces. Planetary mill Retsch PM400 and 250 ml agate jars and agate balls are used. The balls/powder ratio is 5/1. Methanol is used for preventing powder sticking to agate jars and balls. After 20 hours of high energy mixing the barium titanate is the main resulting product and after 50 hours the reaction is completed. Powder obtained is characterized by spherical shapes of grains with dimensions around 50 nanometers. No calcination step is required. Each step of this milling process is followed by morphological and structural characterization of the powder to check the degree of mechanochemical reaction of the raw powders. In order to obtain dense ceramic bodies, the reacted powders are pressed in steel dies, then sintered in alumina crucibles and further mechanically processed to the final desired dimensions. Morphological and structural characterization of sintered ceramics is carried out. After electrodes deposition, ceramic samples are poled by applying a high electric field (30-40kV/cm), which aligns the electric dipoles along the field direction. This is the key step which confers macroscopic piezoelectric properties to ferroelectric
SERVICE PERSONS:
Luminita AMARANDE
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Method for the synthesis of hydrogels with incorporated TiO2 or Fe3O4 nanoparticles
SERVICE DESCRIPTION:
Nanoparticle-hydrogel composites based on 2-hydroxyethyl methacrylate (HEMA) and TiO2 or Fe3O4 nanoparticles are produced via a polymerization process initiated with ammonium persulfate and using ethylene glycol dimethacrylate (EGDMA) as a crosslinking agent.
SERVICE PERSONS:
Traian POPESCU
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Technological Services
Deposition of thin metallic films on various surfaces by physical vapor deposition methods
SERVICE DESCRIPTION:
Surface coating with nanostructured metallic thin films for various applications. Available metals: gold, silver, nickel, titanium, aluminium, molybdenum, tantalum, copper, chromium, vanadium etc. The deposition systems allow for a precise control of film thickness.
SERVICE PERSONS:
Cristina BESLEAGA-STAN
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Adrian ENACHE
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Laser scribing services
SERVICE DESCRIPTION:
The "Perfect Laser PE20W" laser scribing machine has a 20 W YAG laser and can be used for both solar and ceramic cells, but also for scribing other materials.
SERVICE PERSONS:
Adrian ENACHE
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Nanocomposite material synthesis based on carbon black
SERVICE DESCRIPTION:
The nanocomposite carbon black material is prepared using cellulose acetate support matrix. Due to the electrical properties of the carbon black, this material is an excellent choice as a support for the development of sensory platforms. Can be used with commercial supports.
SERVICE PERSONS:
Adrian ENACHE
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Electrochemical sensor on silicon strip
SERVICE DESCRIPTION:
Electrochemical sensors are manufactured on silica strip and are intended to be used in development of electrochemical (bio) sensors for applications in different fields. Besides the classic three-electrode system (reference, auxiliary and working), the sensors also contain two interdigital electrodes.
SERVICE PERSONS:
Adrian ENACHE
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Electrochemical sensor on glass strip
SERVICE DESCRIPTION:
Electrochemical sensors are manufactured on glass strip and are intended to be used in development of electrochemical (bio) sensors for applications in different fields. Besides the classic three-electrode system (reference, auxiliary and working), the sensors also contain two interdigital electrodes.
SERVICE PERSONS:
Adrian ENACHE
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Surface plasmon resonance sensors
SERVICE DESCRIPTION:
The SPR sensors are made of gold with an intermediate titanium thin film.
SERVICE PERSONS:
Adrian ENACHE
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Adapted co-precipitation method for the synthesis of simple- and multi-doped hydroxyapatite (nano)powders
SERVICE DESCRIPTION:
Synthesis of nano-sized hydroxyapatite powders cationically substituted with Zn, Sr, Mg, Ce and/or Ag by the co-precipitation method with applications in bone regeneration medicine.
SERVICE PERSONS:
Daniela PREDOI
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Adapted chemical precipitation method for the synthesis of multifunctional TiO2 nanoparticles
SERVICE DESCRIPTION:
Synthesis of TiO2 nanopowders with variable polymorph phase composition for biomedical and photocatalysis applications
SERVICE PERSONS:
Traian POPESCU
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Adapted co-precipitation method for the synthesis of pure and Fe/Mn doped ZnO nanoparticles
SERVICE DESCRIPTION:
Synthesis of nano-sized ZnO powders pure and doped with Mn/ Fe ions by the co-precipitation method for antibacterial applications
SERVICE PERSONS:
Ioana Dorina VLAICU
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Adapted co-precipitation method for the synthesis of pure and Fe/Mn doped MgO nanoparticles
SERVICE DESCRIPTION:
Synthesis of nano-sized MgO powders pure and doped with Mn/ Fe ions by the co-precipitation method for antibacterial applications
SERVICE PERSONS:
Ioana Dorina VLAICU
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Method for the synthesis of graphene oxide (GO) conjugated with bacterial cellulose and antitumor drugs
SERVICE DESCRIPTION:
Graphene oxide (GO) nanoparticles are conjugated with bacterial cellulose (BC) and antitumor drugs by a method based on the dispersion of GO/BC mixtures in a buffered medium followed by controlled stirring in the presence of antitumor drug molecules.
SERVICE PERSONS:
Claudiu CIOBOTARU
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Hydrothermal method for production of vanadium oxide powders doped with magnetic transition metals
SERVICE DESCRIPTION:
The technology for production of doped vanadium oxide powders is based on the hydrothermal method, where vanadium oxides are mixed with a precursor for magnetic ions in aqueous solution, then, after checking the solubility level, the mixture is stirred and reacts hydrothermally.
SERVICE PERSONS:
Cristian Mihail TEODORESCU
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Gas-aggregation procedure for nanocluster production
SERVICE DESCRIPTION:
The technology is used for the production of nanosized metallic materials (nanoclusters, nanoparticles). It consists of atomic-scale condensation of metal vapors through passing of a rare gas cold cluster beam in a UHV facility. The technology is able to produce tunable sized nanomaterials.
SERVICE PERSONS:
Ovidiu CRISAN
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Procedure for substrate logic conditioning through lithographic pre-patterning
SERVICE DESCRIPTION:
The technology presumes an adapted electron beam lithography technique where a sampling algorithm with predetermined geometries is used. The sampling of the writing fields is conveyed through carefully chosen technological parameters: exposure area, step size and irradiation and dwell times, which are strictly controlled. Prepatterned substrates with rectangular, long range, periodic profiles can thus be obtained with good precision (2% accuracy).
SERVICE PERSONS:
Ovidiu CRISAN
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Research Equipment
Chemistry laboratory
CATALOG NAME:
DESCRIPTION:
The laboratory includes all equipment/reagents normally found in a chemistry laboratory and its technical staff offer scientific support (advice/expertise) and technical support (feasibility/setting up of experiments). Techniques and Equipment: • Analytical devices as HPLC/GC or spectrophotometers • Analytical balance • pH meters • Pipette bulbs • Vacuum filtration device • Laboratory glassware (such as the beaker, reagent bottle, graduated cylinders, volumetric flasks, pipettes, etc) • Ring stands, rings, and clamps, tongs and forceps • Spatulas and scoopulas • Mortars and pestles • Porcelain and alumina crucible • Laboratory thermometer • Autoclaves • Centrifuges • Hot plate and magnetic stirrer • Micro-pipettes • Fume hood (a type of local ventilation device that is designed to limit exposure to hazardous or toxic fumes, vapors or dusts) • Fridge/freezer • Glove box • Ovens • Ultrasonic washers • Desiccators • Water distillation system • Rotary evaporator • Reagents
PRODUCER:
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Electrochemistry laboratory
CATALOG NAME:
DESCRIPTION:
Our electrochemistry laboratory is situated in the RITeC new edifice of NIMP and is equipped with the following instruments: Methrom Autolab potentiostat galvanostat M101; Methrom Autolab potentiostat galvanostat PGSTAT 204; Voltalab PGZ 100; PARSTAT 2273; IVIUM COMPACTSTATh potentiostatl IVIUM COMPACTSTATh potentiostat/bipotentiostat; and ELVEFLOW Plug and Play Microfluidics OB1MK3.
PRODUCER:
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Multi-gun (AJA Phase II J model derived) magnetron sputtering (RF, DC, pulsed DC) deposition system with multiple facilities
CATALOG NAME:
AJA Phase II J
DESCRIPTION:
Equipped with four 2 inch magnetron sputtering guns in con-focal orientation and one 3 inch central magnetron sputtering gun for direct deposition orientation, four AJA International RF generators (1 x 150 W, 2 x 300 W, 1 x 600 W), one one TruPlasma DC 4002 Pulsed DC Power Supply (2 kW Output Power, 800 V Output Voltage, 2.5 A Output Current, 0-100 kHz Output Frequency), and one AJA 750 W DC source. The magnetron guns are designed to assure high uniformity (±1.5 %) on 4 inch wafers. The vacuum system enables attaining a min. 2x10-7 mbar base pressure in the reactor chamber. Facilities: load lock chamber (with cassette for in-situ mask exchange), substrate holder (rotation 0 – 40 rpm, radiant heating up to 850°C, RF/DC biasing, substrate plasma etching), custom planetary style interchangeable substrate carrier capable of indexing up to 6 substrates individually for uniform coating of 3D pieces, quartz crystal thickness monitor, computer control of all processes, closed-loop chiller.
PRODUCER:
AJA International Inc.
PRODUCTION YEAR:
2016
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
RF- and DC-magnetron sputtering deposition system for biocompatible coatings
CATALOG NAME:
UVN-75R1
DESCRIPTION:
Sputtering coating plant dedicated to the implant coating fabrication, equipped with two magnetron large area (diam. 4 inches) guns, a substrate clean-up position by glow discharge, in situ substrate heating and biasing facilities, and planetary rotation of the substrate.
PRODUCER:
VACMA
PRODUCTION YEAR:
1972
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (0 kb)
Pull-out tensile adhesion testers
CATALOG NAME:
Models: GM01/6.3kN & PAThandy/1kN manual tensile pull testers
DESCRIPTION:
Manual hydraulic tensile adhesion testers dedicated to the measure of bonding strength of thin films, coatings, varnishes, and paints. The testing systems and method comply with ISO 4624, ASTM D 4541, EN 1542 and ASTM C633 standards.
PRODUCER:
DFD Instruments
PRODUCTION YEAR:
2008
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Download data sheet file (2356.49 kb)
X-ray diffractometer in powder setting
CATALOG NAME:
D8-ADVANCE
DESCRIPTION:
The goniometer is configured in Bragg-Brentano parafocusing geometry, with vertical goniometer. The diffractometer is equipped with a ceramic, copper target X-ray tube. A molybdenum target tube is also available, if high scattering vector range measurement is needed. Two detectors are available: a NaI(Tl) scintillation counter for conventional measurements, and a linear detector (LynxEye-type) with an angular window of 2°, providing a collection rate about 100 times higher than that of the scintillation counter, designed for high speed, quality measurements. A temperature chamber MRI TC-Wide Range for in situ measurements between -180°C and 450°C.
PRODUCER:
BRUKER-AXS
PRODUCTION YEAR:
2007
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
X-ray diffractometer in thin films setting
CATALOG NAME:
D8-ADVANCE
DESCRIPTION:
The X-ray diffractometer has a vertical goniometer, and is equipped with a copper target X-ray tube and scintillation detector. The goniometer setting (a Göbel mirror, and a Ge (220) double monochromator) provides a parallel X-ray beam.
PRODUCER:
BRUKER-AXS
PRODUCTION YEAR:
2006
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Fourier Transform infrared spectrometer
CATALOG NAME:
Perkin-Elmer Spectrum BX II
DESCRIPTION:
The spectrometer performs measurements in the transmission/ATR mode (Diamond-ZnSe, ZnSe, and Ge crystals). Wavelength Range: 7800 to 350 cm-1. It provides fast throughput, rapid identification processing and quantification of samples, as well as accurate and dependable results. Built-in validation saves time and money. Exhaustive integrity tests are performed at three levels to ensure that it is working correctly, and that the data is both properly collected and accurate.
PRODUCER:
PERKIN-ELMER
PRODUCTION YEAR:
2004
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
X-ray photoelectron spectrometer
CATALOG NAME:
AXIS ULTRA DLD
DESCRIPTION:
• The XPS equipment includes an airlock connected with high-pressure cell; • X-ray source: Al K alpha/alpha monochromatized L Ag single crystal using a focus with the spot size of 0.7 mm, Al K alpha spectral resolution (1.2) 0.2 eV; • Electron analyzer: hemispherical analyzer with a reference intensity of over 50,000 counts per second (cps) with a maximum; spectral resolution of 0.7 eV, standard line of Ag 3d5 / 2 Ag metal or C 1s on the chart; • Sample treatment at high pressures and temperatures (treatment at maximum pressures of 5 bar, and at temperatures up to; 300°C and at a pressure of max. 1 bar in conditions of temperature up to 1000°C); • Microscopic system with CCD camera for monitoring the position of the sample; • Sample cleaning ion source, voltage 2 kV, the current 1mA; • Vacuum limit: 5 x 10-10 mbar; • Possibility to heat/cool the sample in the analysis chamber in (- 100°C, 500°C).
PRODUCER:
KRATOS ANALYTICAL
PRODUCTION YEAR:
2015
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Scanning electron microscope (SEM) with Energy-dispersive X-ray spectroscopy attachment
CATALOG NAME:
SEM - Carl Zeiss EVO 50 XV & EDXS - Bruker-AXS 133eV XFlash 4010
DESCRIPTION:
SEM allows for morphological determinations: shape and particles size analysis of micro- and nano-objects, surfaces and interfaces. EDXS allows for quantitative elemental composition determinations and elemental cartography/distributions.
PRODUCER:
Carl Zeiss / Bruker-AXS
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Raman spectroscopy
CATALOG NAME:
FT Raman spectrophotometer RFS 100/S
DESCRIPTION:
Excitation source: YAG: Nd laser (1064 nm), power 500 mW, horizontally polarized (H), resolution 1 cm-1, spectral range 50-3600 cm-1 (Stokes shift), -100…-2000 cm-1 (anti-Stokes shift), backscattering measuring geometry.
PRODUCER:
Bruker
PRODUCTION YEAR:
2005
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
High-resolution transmission electron microscope (TEM)
CATALOG NAME:
JEOL JEM ARM 200F
DESCRIPTION:
Configuration: · Field Emission Gun (FEG); · Cs-corrector for STEM mode; · STEM Unit; · EDS Unit: JEOL JED-2300T; · GIF (Gatan Image Filter): Gatan Quantum SE; · CCD Cameras: wide angle: Gatan Orius 200D, bottom mounted: Gatan Ultrascan 1000XP, GIF camera: Gatan Ultrascan 1000F. Working modes: · CTEM, HRTEM, STEM BF, STEM ADF, STEM HAADF, SAED, nano-ED, CBED, EDS, EELS, EFTEM, EELS-SI; Technical specifications: · Accelerating voltages: max. 200 kV; · TEM magnification: 50 – 2 000 000 × ; · TEM resolution: 0.19 nm; · STEM magnification: 200 – 150 000 000 × ; · STEM-HAADF resolution: 0.08 nm; · EDS: - energy resolution EDS: 131,4 eV (Mn-Ka) - in TEM mode; - in STEM mode: spot, line profile or 2D mapping; · EELS – energy resolution 0.7 eV.
PRODUCER:
JEOL
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Atomic force microscope (AFM)
CATALOG NAME:
NT-MDT INTEGRA Probe NanoLaboratory system
DESCRIPTION:
Works in contact and non-contact mode; cantilever: a high-resolution silicon NT-MDT NSG01 having a tetrahedral tip, with the last 500 nm from tip apex cylindrical. The typical curvature radius is 6 nm (at most 10 nm guaranteed by the producer). The tip height is 14-16 nm, the cone angle at the apex is 7-10°, whilst the aspect ratio is up to 7:1.
PRODUCER:
NT-MDT
PRODUCTION YEAR:
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Phone:
+40-(0)21-2418100
Fax:
Atomistilor
,
405A
,
Magurele
077125
,
Ilfov
Romania
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